问题：帮忙查一下这个物质的合成方法？？谢谢
类型：求助 (悬赏分:3分)
提问：wenchunlin
等级：▲▲▲
版块：有机化学问题(jimuwei,fpcwin1211,netpanda,yjgzfl,Ftian,)
信誉：97%
回复：4
阅读：420
时间：2006-02-26 21:05:21 编辑加入/取消收藏订制/取消短消息举报该贴

权限大的老师帮忙查一下这个物质的合成方法哦？！谢谢

回复人：ecustlian,▲▲▲ (相互学习,共同提高) 时间：2006-02-26 21:32:35 编辑

1楼

Copyright (c) 1988-2005, Beilstein Institut zur Foerderung der Chemischen Wissenschaften licensed to Beilstein GmbH and MDL Information Systems GmbH. All rights reserved.
Reaction (Beilstein(2005/03):Reactions:Q01 hit 3, RX.ID 4240595)
Reaction ID 4240595
Reactant BRN 607605 2-methoxy-benzoyl chloride

103222 thiophene
Product BRN 142759 (2-hydroxy-phenyl)-thiophen-2-yl-methanone
No. of Reaction Details 1
Find similar reactions click here

Field Availability List (Beilstein(2005/03):Reactions:Q01 hit 3, RX.ID 4240595)
Code Field Name Occ.
RX Reaction Details 1

Reaction Details (Beilstein(2005/03):Reactions:Q01 hit 3, RX.ID 4240595)
Reaction Classification Preparation
Reagent AlCl3
Solvent CH2Cl2
Time 2 hour(s)
Other Conditions Heating
Note 1 Yield given
Ref. 1 5968679; Journal; Varache-Lembege, Martine; Nuhrich, Alain; Renard, Pierre; Duboudin, Francoise; Vercauteren, Joseph; Devaux, Guy; ARPMAS; Arch.Pharm.(Weinheim Ger.); EN; 328; 5; 1995; 417-424.

RX.ID=4240595:

回复人：ecustlian,▲▲▲ (相互学习,共同提高) 时间：2006-02-26 21:32:56 编辑

2楼

Beilstein Data: Copyright (c) 1988-2005, Beilstein Institut zur Foerderung der Chemischen Wissenschaften licensed to Beilstein GmbH and MDL Information Systems GmbH. All rights reserved.
Reaction (Beilstein(2005/03):Reactions:Q01 hit 2, RX.ID 1751053)
Reaction ID 1751053
Reactant BRN 132326 thiophene-2-carboxylic acid phenyl ester
Product BRN 142759 (2-hydroxy-phenyl)-thiophen-2-yl-methanone
No. of Reaction Details 1
Find similar reactions click here

Field Availability List (Beilstein(2005/03):Reactions:Q01 hit 2, RX.ID 1751053)
Code Field Name Occ.
RX Reaction Details 1

Reaction Details (Beilstein(2005/03):Reactions:Q01 hit 2, RX.ID 1751053)
Reaction Classification Preparation
Yield 30 percent (BRN=142759)
Reagent AlCl3
Temperature 140 - 160 C
Ref. 1 5860360; Journal; Thakar, K. A.; Padhye, A. M.; JICSAH; J. Indian Chem. Soc.; EN; 61; 8; 1984; 715-716.

RX.ID=1751053:

回复人：ecustlian,▲▲▲ (相互学习,共同提高) 时间：2006-02-26 21:33:13 编辑

3楼

Beilstein Data: Copyright (c) 1988-2005, Beilstein Institut zur Foerderung der Chemischen Wissenschaften licensed to Beilstein GmbH and MDL Information Systems GmbH. All rights reserved.
Reaction (Beilstein(2005/03):Reactions:Q01 hit 5, RX.ID 8711659)
Reaction ID 8711659
Reactant BRN 8682232 thiophene-2-sulfonic acid 2-formyl-phenyl ester
Product BRN 142759 (2-hydroxy-phenyl)-thiophen-2-yl-methanone
No. of Reaction Details 1
Find similar reactions click here

Field Availability List (Beilstein(2005/03):Reactions:Q01 hit 5, RX.ID 8711659)
Code Field Name Occ.
RX Reaction Details 1

Reaction Details (Beilstein(2005/03):Reactions:Q01 hit 5, RX.ID 8711659)
Reaction Classification Preparation
Yield 48 percent (BRN=142759)
Reagent di-tert-butyl peroxide
Solvent chlorobenzene
Time 24 hour(s)
Other Conditions Heating

RX.ID=8711659:

回复人：wenchunlin,▲▲▲ (欢迎光临我的论坛http://www.happychem.com.cn/bbs) 时间：2006-02-26 21:50:57 编辑	4楼
已经打分了。

得分人：ecustlian-3,

问题讨论没有结束...

您尚未进入本论坛,登录之后才可以回贴

6msec