问题：求求2,5-二氯对苯二甲酸
类型：求助 (悬赏分:3分)
提问：nakata
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时间：2006-03-13 11:14:55 编辑加入/取消收藏订制/取消短消息举报该贴

求2,5-二氯对苯二甲酸的数据资料及合成文献？

回复人：tangyyer,★★★★★ (有空来逛逛my blog: http://tangyyer.blog.hexun.com) 时间：2006-03-13 13:37:33 编辑

1楼

Molecular Formula: C8H4Cl2O4
Molecular Weight: 235.023
Accurate Mass: 233.948664
Percentage Composition: C 40.88%; H 1.72%; Cl 30.17%; O 27.23%
Use/Importance: Polymerisation substrate
Physical Description: Needles (H2O) or by subl.
Melting Point: Mp 306 (303)

Cachia, M. et al., Bull. Soc. Chim. Fr., 1958, 1418
Neel, J. et al., Bull. Soc. Chim. Fr., 1967, 3377, (synth)
Otto, J. et al., Pol. J. Chem. (Rocz. Chem.), 1967, 41, 261, (synth)
Japan. Pat., 1974, 74 107 397; CA, 84, 123286q, (synth)

回复人：maurice,★★ (自信,乐观,富于激情,积极面对人生) 时间：2006-03-13 14:07:22 编辑	2楼
对苯二甲酸氯化

回复人：nakata,▲▲▲▲▲ () 时间：2006-03-13 17:23:11 编辑	3楼
顶啊

回复人：ecustlian,▲▲▲ (相互学习,共同提高) 时间：2006-03-13 19:24:30 编辑

4楼

Reaction Classification Preparation (half reaction)
Ref. 1 3774655; Journal; Duhamel; ANCPAC; Ann.Chim.(Paris); 8; 13; 1963; 315,338.
Ref. 2 3809216; Journal; Kirrmann et al.; COREAF; C. R. Hebd. Seances Acad. Sci.; 250; 1960; 3190.
Ref. 3 3934248; Journal; Diembeck; Eibl; CPLIA4; Chem. Phys. Lipids; 24; 1979; 237,240.
Ref. 4 4142355; Journal; Below; Poljakowa; ZVKOA6; Zh. Vses. Khim. O'va im. D. I. Mendeleeva; 10; 1965; 110.
Ref. 5 4490440; Patent; Aldr.-Boranes Inc.; US 3978140; 1976; Chem.Abstr.; EN; 85; 192339.
Ref. 6 5226634; Journal; Belov; Poljakova; JOCYA9; J.Org.Chem.USSR (Engl.Transl.); 3; 1967; 1354; ZORKAE; Zh. Org. Khim.; 3; 1967; 1392.

回复人：ecustlian,▲▲▲ (相互学习,共同提高) 时间：2006-03-13 19:24:46 编辑	5楼
Reaction Classification Preparation (half reaction) Ref. 1 4241227; Journal; Otto; Paluch; ROCHAC; Rocz. Chem.; 46; 1972; 1551,1552. Ref. 2 4460805; Journal; Ballester et al.; JACSAT; J. Am. Chem. Soc.; 82; 1960; 4254,4256. Ref. 3 5311858; Journal; Otto; Paluch; ROCHAC; Rocz. Chem.; 41; 1967; 261.

回复人：ecustlian,▲▲▲ (相互学习,共同提高) 时间：2006-03-13 19:25:12 编辑

6楼

Beilstein Data: Copyright (c) 1988-2005, Beilstein Institut zur Foerderung der Chemischen Wissenschaften licensed to Beilstein GmbH and MDL Information Systems GmbH. All rights reserved.
Reaction (Beilstein(2005/03):Reactions:Q02 hit 9, RX.ID 7299533)
Reaction ID 7299533
Reactant 2.5-dichloro-cymene
Product BRN 2115355 2,5-dichloro-terephthalic acid
No. of Reaction Details 1
Find similar reactions not available

Field Availability List (Beilstein(2005/03):Reactions:Q02 hit 9, RX.ID 7299533)
Code Field Name Occ.
RX Reaction Details 1

Reaction Details (Beilstein(2005/03):Reactions:Q02 hit 9, RX.ID 7299533)
Reaction Classification Preparation (half reaction)
Reagent nitric acid
Temperature 190 C
Other Conditions im geschlossenen Rohr
Note 1 Handbook
Ref. 1 1666559; Journal; Bocchi; GCITA9; Gazz. Chim. Ital.; 26 II; 1896; 405.

RX.ID=7299533:

--------------------------------------------------------------------------------
Beilstein Data: Copyright (c) 1988-2005, Beilstein Institut zur Foerderung der Chemischen Wissenschaften licensed to Beilstein GmbH and MDL Information Systems GmbH. All rights reserved.
Reaction (Beilstein(2005/03):Reactions:Q02 hit 10, RX.ID 7299534)
Reaction ID 7299534
Reactant 2.5-dichloro-p-cymene
Product BRN 2115355 2,5-dichloro-terephthalic acid
No. of Reaction Details 1
Find similar reactions not available

Field Availability List (Beilstein(2005/03):Reactions:Q02 hit 10, RX.ID 7299534)
Code Field Name Occ.
RX Reaction Details 1

Reaction Details (Beilstein(2005/03):Reactions:Q02 hit 10, RX.ID 7299534)
Reaction Classification Preparation (half reaction)
Reagent nitric acid
Note 1 Handbook
Ref. 1 1541251; Journal; Wheeler; Giles; JACSAT; J. Am. Chem. Soc.; 44; 1922; 2608.

RX.ID=7299534:

--------------------------------------------------------------------------------
Beilstein Data: Copyright (c) 1988-2005, Beilstein Institut zur Foerderung der Chemischen Wissenschaften licensed to Beilstein GmbH and MDL Information Systems GmbH. All rights reserved.
Reaction (Beilstein(2005/03):Reactions:Q02 hit 11, RX.ID 7299535)
Reaction ID 7299535
Reactant 2.5-dichloro-p-xylene
Product BRN 2115355 2,5-dichloro-terephthalic acid
No. of Reaction Details 1
Find similar reactions not available

Field Availability List (Beilstein(2005/03):Reactions:Q02 hit 11, RX.ID 7299535)
Code Field Name Occ.
RX Reaction Details 1

Reaction Details (Beilstein(2005/03):Reactions:Q02 hit 11, RX.ID 7299535)
Reaction Classification Preparation (half reaction)
Note 1 Handbook
Ref. 1 1682800; Journal; Wheeler; Morse; JACSAT; J. Am. Chem. Soc.; 46; 1924; 2574.

RX.ID=7299535:

回复人：nakata,▲▲▲▲▲ () 时间：2006-03-13 20:32:54 编辑	7楼
有文献没有啊？直接连接的

回复人：nakata,▲▲▲▲▲ () 时间：2006-03-14 12:56:06 编辑	8楼
ding

回复人：nakata,▲▲▲▲▲ () 时间：2006-03-16 19:23:36 编辑	9楼
我再顶

回复人：tangyyer,★★★★★ (有空来逛逛my blog: http://tangyyer.blog.hexun.com) 时间：2006-03-17 08:23:38 编辑	10楼
直接连接?这些都需要到图书馆下载的，找找代理或者ez，自己去下吧。

回复人：nakata,▲▲▲▲▲ () 时间：2006-03-17 11:18:00 编辑	11楼
我下不了的,麻烦哪位老兄,帮我下, nakatakaori@sina.com

回复人：nakata,▲▲▲▲▲ () 时间：2006-03-18 17:22:46 编辑	12楼
已经打分了。

得分人：tangyyer-1,ecustlian-1,

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