问题：求助：β-二甲氨基丙腈及丁腈的相关资料！
类型：求助 (悬赏分:3分)
提问：dashing
等级：★
版块：有机化学问题(jimuwei,fpcwin1211,netpanda,yjgzfl,Ftian,)
信誉：100%
回复：3
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时间：2006-04-05 23:53:39 编辑加入/取消收藏订制/取消短消息举报该贴

求助这两种物质的物理性质和化学性质，合成方法及应用等资料，越详细越好，谢谢！

回复人：tangyyer,★★★★★ (有空来逛逛my blog: http://tangyyer.blog.hexun.com) 时间：2006-04-06 23:39:45 编辑

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β-二甲氨基丙腈:
Property Value Condition Note
Boiling Point 173 癈 NLM
Boiling Point 173 癈 SRC
Boiling Point 76-77 癈 Press: 24 Torr (1) IC
Boiling Point 72 癈 Press: 19 Torr (2) CAS
Density 0.8705 g/cm3 Temp: 20 癈 NLM
Melting Point -44.2 癈 NLM
Refractive Index 1.4360 Wavlen: 589.3 NLM
nm
Temp: 20 癈
Refractive Index 1.4259 Temp: 18 癈 (1) IC

丁腈:
Property Value Condition Note
Boiling Point 117.9 癈 (1) CAS
Boiling Point 117.6 癈 SRC
Boiling Point 117.5 癈 Press: 760 Torr NLM
Boiling Point 117.4 癈 (2) CAS
Boiling Point 117 癈 Press: 760 Torr (3) IC
Boiling Point 116-118 癈 NIOSH
Boiling Point 116-117 癈 (4) CAS
Boiling Point 116-117 癈 Press: 755 Torr (5) IC
Boiling Point 116 癈 Press: 750 Torr (6) IC
Boiling Point 116 癈 Press: 750 Torr (7) IC
Boiling Point 115 癈 (8) CAS
Boiling Point 115 癈 Press: 748 Torr (9) IC
Boiling Point 114-118 癈 Press: 760 Torr (10) IC
Boiling Point 114 癈 (11) CAS
Boiling Point 113 癈 Press: 760 Torr (12) CAS
Boiling Point 110 癈 Press: 637 Torr (13) CAS
Boiling Point 110 癈 Press: 760 Torr (12) CAS
Density 0.8091 g/cm3 Temp: 0 癈 NLM
Density 0.8 g/cm3 NIOSH
Density 0.7891 g/cm3 Temp: 20 癈 (4) CAS
Density 0.78183 g/cm3 Temp: 30 癈 (1) CAS
Med. Lethal Dose-LD50 220 mg/kg Organism: rat (21) CAS
Route: oral
Med. Lethal Dose-LD50 50 mg/kg Organism: (21) CAS
mouse
Route:
intraperitoneal
Melting Point -111.9 癈 SRC
Melting Point -112 癈 (8) CAS
Melting Point -112 癈 NIOSH
Melting Point -112 癈 NLM
Proton NMR Spectrum See full text (14) CAS
Proton NMR Spectrum See full text (15) CAS
Proton NMR Spectrum See full text (10) IC
Proton NMR Spectrum See full text (6) IC
Proton NMR Spectrum See full text (18) IC
Proton NMR Spectrum See full text (22) CAS
Proton NMR Spectrum See full text (5) IC
Proton NMR Spectrum See full text (23) IC
Proton NMR Spectrum See full text (7) IC
Refractive Index 1.38623 Temp: 15 癈 (1) CAS
Refractive Index 1.3851 Temp: 25 癈 (7) IC
Refractive Index 1.3849 Temp: 25 癈 (6) IC
Refractive Index 1.3848 Temp: 25 癈 (5) IC
Refractive Index 1.3845 Wavlen: 589.3 (4) CAS
nm
Temp: 20 癈
Refractive Index 1.3840 Temp: 20 癈 (9) IC
Refractive Index 1.38385 Wavlen: 589.3 NLM
nm
Temp: 20 癈

回复人：tangyyer,★★★★★ (有空来逛逛my blog: http://tangyyer.blog.hexun.com) 时间：2006-04-06 23:43:16 编辑	2楼
β-二甲氨基丙腈的合成见：WO 9619998；US 5334745；US 5237088；EP 353599；EP 352504；JP 47003809。丁腈的合成见：WO 2003099211；US 5847230；WO 9403435；EP 231138。

回复人：dashing,★ (油田化学/高分子合成 http://bbs.petroren.com/?fromuid=9653) 时间：2006-04-24 10:17:58 编辑	3楼
已经打分了。

得分人：tangyyer-2,

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