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问题:请帮找一下,下面两个化合物的合成,谢谢了.
类型:求助 (悬赏分:3分)
提问:waltjf
等级:
版块:有机化学问题(jimuwei,fpcwin1211,netpanda,yjgzfl,Ftian,)
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时间:2006-08-15 06:07:18  编辑    加入/取消收藏    订制/取消短消息    举报该贴    

化合物1:3-Amino-5-bromobenzotrifluoride,CAS:54962-75-3

化合物2: 2,3,3,5-Tetramethyl-3H-indole CAS:25981-82-2

谢谢.

[该帖子已被waltjf在2006-8-16 6:36:45编辑过]
回复人:waltjf, (农药工业化工艺开发) 时间:2006-08-15 12:44:36   编辑 1楼
没有人帮忙吗?


回复人:Phyyx, (基础比较差) 时间:2006-08-15 14:01:31   编辑 2楼
你有CAS号
就上beilstein,scifinder
上查查看吧
应该很多


回复人:zhaijf,▲▲▲▲ (有机化学真高深) 时间:2006-08-15 17:15:18   编辑 3楼
Compound 1:
Finger, G.C. et al., J.A.C.S., 1944, 66, 1972
Benkeser, R.A. et al., J.A.C.S., 1952, 74, 3011


回复人:waltjf, (农药工业化工艺开发) 时间:2006-08-16 06:30:21   编辑 4楼
化合物2帮我查一下,我一起加分 .


回复人:Phyyx, (基础比较差) 时间:2006-08-16 10:57:36   编辑 5楼
Zimmermann, Thomas; Hennig, Lothar. Ring transformations of heterocyclic compounds. XXII [1]. Pyrido[1,2-a]indolium salts from 2-methyl-3H-indoles by pyrylium mediated three carbon annelation. Journal of Heterocyclic Chemistry (2002), 39(2), 263-269. CODEN: JHTCAD ISSN:0022-152X. CAN 137:247583 AN 2002:389414 CAPLUS


Fujita, Shigeo; Sasaki, Nobuaki; Wada, Sayuri; Iwasaki, Yasuhisa. Method for preparation of indolenine compounds by amination of 3-bromo-3-methylbutan-2-one with anilines and cyclization of 3-anilino-3-methyl-2-butanone. Jpn. Kokai Tokkyo Koho (2002), 17 pp. CODEN: JKXXAF JP 2002088060 A2 20020327 CAN 136:263095 AN 2002:233088 CAPLUS


Sackus, A.; Martynaitis, V. Unexpected formation of the 6,7,13,13a-tetrahydro-15H-1,4-diazepino[1,7-a:4,5-a']diindole system in the reaction of 2,3,3-trimethyl-3H-indole with chloroacetonitrile. Chemistry of Heterocyclic Compounds (New York, NY, United States)(Translation of Khimiya Geterotsiklicheskikh Soedinenii) (2001), 37(2), 256-258. CODEN: CHCCAL ISSN:0009-3122. CAN 135:272942 AN 2001:576667 CAPLUS

Fukahori, Choko; Maeda, Shuichi; Takuma, Juki; Iizuka, Yoshiaki. Method for producing indoline compounds. Jpn. Kokai Tokkyo Koho (1995), 6 pp. CODEN: JKXXAF JP 07173156 A2 19950711 Heisei. CAN 123:256517 AN 1995:835608 CAPLUS

Sackus, A.; Degutis, J.; Medeksiene, H. Synthesis of 11,12,12a,13-tetrahydro-6H-indolo[1,2-b][2,4]benzodiazepine derivatives. Khimiya Geterotsiklicheskikh Soedinenii (1990), (6), 815-17. CODEN: KGSSAQ ISSN:0453-8234. CAN 114:42751 AN 1991:42751 CAPLUS

Sackus, A.; Degutis, J.; Urbonavicius, A. Synthesis and investigation of 5a,6-dihydro-12H-indolo[2,1-b][1,3]benzoxazine derivatives. Khimiya Geterotsiklicheskikh Soedinenii (1989), (5), 672-6. CODEN: KGSSAQ ISSN:0453-8234. CAN 112:55742 AN 1990:55742 CAPLUS


Degutis, J.; Sackus, A.; Urbonavicius, A. Reaction of 2,3,3-trimethyl-3H-indole with haloacetamides. Synthesis of 1,2,3,9a-tetrahydro-9H-imidazo[1,2-a]indol-2-ones. Khimiya Geterotsiklicheskikh Soedinenii (1985), (7), 933-5. CODEN: KGSSAQ ISSN:0453-8234. CAN 103:160443 AN 1985:560443 CAPLUS


回复人:Phyyx, (基础比较差) 时间:2006-08-16 10:59:07   编辑 6楼
上面是化合物2的一些资料
我就是用你给的CAS:25981-82-2查的
不知道对不对,内容我也没仔细看


回复人:waltjf, (农药工业化工艺开发) 时间:2006-08-16 16:14:05   编辑 7楼
已经打分了。


回复人:simonsun, (医药中间体,原料药) 时间:2007-07-17 10:14:57   编辑 8楼
,3,3,5-Tetramethyl-3H-indole  CAS:25981-82-2 这个我可以提供产品


得分人:Phyyx-2,zhaijf-3,


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